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1 article(s) from Rey, Yannick P.

Modulating NHC catalysis with fluorine

Yannick P. Rey and
Ryan Gilmour

Beilstein J. Org. Chem. 2013, 9, 2812–2820, doi:10.3762/bjoc.9.316

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Graphical Abstract

Figure 1: Exploring the effect of fluorine incorporation in triazolium pre-catalysts (2) for the enantioselec...

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Figure 2: Target triazolium salts 5–10 for this study. The synclinal-endo conformation of 5 is shown [18]. Only t...

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Scheme 1: Synthesis of the difluorinated triazolium salt 7 starting from commercially available N-Boc-trans-4...

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Scheme 2: Synthesis of the monofluorinated triazolium salt 8.

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Scheme 3: Synthesis of the trifluoromethylated and non-fluorinated pre-catalysts 9 and 10 for control studies....

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Figure 3: X-ray crystal structures of triazolium salts 5·BF₄⁻, 6·BF₄⁻ and 7·BF₄⁻ [42]. The tetrafluoroborate coun...

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Figure 4: An overview of the molecular editing approach to catalyst development.

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Published 06 Dec 2013

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